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Contents of volume 49
CONTENTS
OF VOLUME
49
NUMBER 1, AUGUST 1982 C. V. LAGODZINSKAYA AND I. Yu. KLIMENKO. Measurement
tion for Magnetic Susceptibility with Solenoidal Magnet trometers .._._..._._._..._._..............._............._..
and CorrecNMR SpecE.
. J. OSTEN AND R. RADEGLIA. Spin Dynamics
of an AX System in FTNMR Experiment by the Example of the {‘H}-CW-Off-Resonance Decoupled r3C NMR Spectrum of Chloroform
JAMES F. HAW, T. E. GLASS, AND H. C. DORN. Conditions
Flow FT-‘H
NMR
Measurements
for Quantitative under Repetitive Pulse Conditions
8 22
DAVID T. PEGG, M. ROBIN BENDALL, AND DAVID M. DODDRELL. Ran-
domization
of Spins in Heteronuclear
Pulse Sequences
32
P. W. FRANCE AND M. WADSWORTH. Satellites and Shoulders in the NMR
“B Resonance of Borate Glass
48
KEIICHI OHNO. Application
of ESR Imaging to a Continuous Flow Method for Study on Kinetics of Short-Lived Radicals
J. N. HERAK, ALKA VELENIK, AND C. A. MCDOWELL. An ENDOR Study of Long-Range Spin Interactions in Molecular Crystals. II. The 5-Thymy1 Radical in a Single Crystal of Thymidine .. .. .. T. VAANANEN, J. JOKISAARI, AND J. LOUNILA. The Structure and Orientational Behavior of o&o-Difluorobenzene in Nematic Liquid Crystals
56
64 73
HENRY ZELDES AND RALPH LIVINGSTON. The Use of Spectral Simulations
for the Assay of Radical Concentrations R. C. BOWMAN, JR., AND W.-K.
for Second-Moment
by ESR
RHIM. A Simple Magic-Echo
84 Sequence
Measurements
93
P. DwBors MURPHY, T. TAKI, B. C. GERSTEIN, P. M. HENRICHS, AND D. J. MASSA. Shielding Anisotropies of 13C in Poly(ethylene terephthalate) . . ...__._..._....__.....__._.___....,.._.,__.,.,._ D. A. TORCIIIA AND ATTILA SZABO. Spin-Lattice
Relaxation
99
in Solids
P. J. HORE, M. R. EGMOND, H. T. EDZES, AND R. KAPTEIN. Cross-Re-
laxation Effects in the Photo-CIDNP Spectra of Amino Acids and Proteins . . .._......._.._.._...................._.._..._.._..
122
NOTES B. BL~MICH AND D. ZIESSOW. Skyline Projections in Two-Dimensional
NMR
Spectroscopy
P. N. TUTUNJIAN AND J. S. WAUGH. The Anisotropy
of the 31P-3iP
Indirect Nuclear Coupling G. HURST, K. KRAFT, R. SCHULTZ, AND R. KREILICK. Radiofrequency
Coil Construction
for a Bruker/IBM
ENDOR
Cavity
STEVEN L. PATT. Pulse Strategies for the Suppression of Acoustic Ring-
ing ..~.~.~....~~.~~~~~..~..~.....~~~~
., ._..
_. _.......
COMMUNICATIONS S. J. KARLIK, G. A. ELGAVISH, R. P. PILLAI, AND 6. L. EICHWORN.
Aluminum-27 NMR Studies of Al(III)-Phosphate Aqueous Solution .._ _........ __ . . . A. N. GARROWAY. Magic-Angle
Complexes in __ .._
Sample Spinning of Liquids
MICHAEL BATLEY AND JOHN W. REDMOND. 31PNMR
Reference Stan-
dards for Aqueous Samples DAVID L. TURNER. Carbon-13
Quantum
Coherence
Autocorrelation NMR Using Double~~.~~.~......~.~...~~~~~~..~.~.~_..~.
BOOK REVIEWS Ferromagnetodynamics: The Dynamics of Magnetic Bubbles, Domains and Domain Wails. T. H. O’Dell Specialist Periodical Reports. Spectroscopic Properties of Inorganic and Organometallic Compounds. D. M. Adams and E. A. V. Ebs-
worth, Senior Reporters Computer
Networks
in the Chemical
Laboratory.
Edited by George
C. Levy and Dan Terpstra NUMBER 2, SEPTEMBER 1982 DAVID M. DODDRELL, DAVID T. PEGG, AND M. ROIXN BENDALL.
stochastic J Cross-Polarization
in Liquids
.JOSEP~~ GRANOT. Resolution Effects in Spin-Lattice
surements
Relaxation Time
._..r.,,.._.___...._......__.........I._..........
THOMAS HERRLING, NORBERT KLIMES, WOLFGANG KARTHE, UWE EwERT, AND BERND EBERT. EPR Zeugmatography with Modulated ag-
netic Field Gradient PXOTR FAJER AND DEREK MARSH. Microwave
and Modulation Field homogeneities and the Effect of Cavity Q in Saturation Transfer E Spectra. Dependence on Sample Size
212
T. LIONEL, J. R. MORTON, AND K. F. PRESTON. The EPR Spectrum
of 225
Qs(CO)~+ Trapped in a Single Crystal of Cr(CO), W. SCHAJOR, U. HAEBERLEN, AND J. TEGENFELDT. Identification Characterization of the Motion of Water Molecules in Normal Deuterated Pyromellitic Acid Dihydrate
and and 233
The Interaction of Cobalt with Glycerophosphoryl Glycerol and Phosphatidyl Glycerol Bilayer Membranes
ALAN C. MCLAUGHLIN.
JOSEPH GRANOT. Paramagnetic
Relaxation
in Dipolar-Coupled
246
Homonu-
clear Spin Systems
251
T. C. NG, W. T. EVANOCHKO, R. N. HIRAMOTO, V. K. GHANTA, M. LILLY, A. J. LAWSON, T. H. CORBETT, J. R. DURANT, AND J. GLIcKSON. 31P NMR Spectroscopy of in Viva Tumors
271
B. B. SHARMA, G. CHIDICHIMO, A. SAUPE, H. CHANG, AND G. H. BROWN. Linewidth Analysis of the Proton Resonance Spectrum of Benzene in a Nematic Solution
287
W. WOLNEY FILHO, R. L. HAVILL, AND J. M. TITMAN. Nuclear elaxation in Molten Alkali Nitrates
2%
Spin
BRETT AND D. T. EDMONDS. 170 and ‘H NQR Study of Solid Meth-
anol Near Its Melting
Temperature
SOOK LEE, D. P. AMES, AND J. M. PUTNAM. Occurrence
of Abnormal Divergence Peaks in Axially Symmetric EPR Hyperhine Powder Spectra ..__....__.....__._...__..._._...._____._..__.___,,_._.
312
NOTES
9. HENNIG AND H. H. LIMBACH. Magnetization Transfer in the Rotating Frame: A New Simple Kinetic Tool for tbe Determination of Rate Constants in the Slow Chemical Exchange Range
322
NICHOLAS ZUMBULYADIS. Suppression of the Spinner Signal in Magic-
Angle-Spinning
NMR
A. LOEWENSTEIN. NMR
329 Study of the Azide Ion
332
ANTHONY S. SERIANNI AND ROBERT BARKER. 13C Spin-Lattice
laxation Times of [ l-‘3C]-Enriched
Re-
Carbohydrates
W. T. DIXON, JACOB SCHAEFER, M. D. SEFCIK, E. 0. STEJSKAL, AND R. A. MCKAY. Total Suppression of Sidebands in CPMAS C- 13 NMR ,.,......__..........___...__......._...___._.._. BRUCE COOK AND I. J. LOWE. A Large-Inductance,
High-Q, Series-Tuned Coil for NMR
335
341
High-Frequency, 346
COMMUNICATIONS A. SAMOSON, E. KUNDLA, AND E. LIPPMAA. High Resolution
NMR
of Quadrupolar
MAS-
Nuclei in Powders
ERHARD HAUPT. A Timesaving
Method to Determine the Length of a 90” Pulse ~~~...~~.~~.~~.~~~.~...~~~~........~.~~~...~~
T. TERAO, H. MIURA, AND A. SAIKA. Measurements of the 13C--lH Coupling Constants in Solid Adamantane: Resolution Enhancement by Multiple-Pulse Decoupling
365
P. DUBOIS MURPHY. Elimination of the Power Mismatch ments in Cross-Polarization NMR
368
Require-
NUMBER 3, OCTOBER ‘1, 1982 RONALD CROUCH, STUART HURLBERT, AND ARIS RAGOUZEOS. An Iter-
ative Linear Method for Calculation
of Spin-Lattice
Relaxation Times
CLAYDEN AND R. J. P. WILLIAMS. Peptide Group Shifts
371 383
Conformational Analysis of and Glycyl-L-Histidine from Nuclear-Nuclear . Spin Relaxation
BRUNT PERLY AND CLAUDE CHACHATY.
L-Alanyl-L-Tryptophan and Electron-Nuclear
397
MIRKO I. HROVAT, CHESTER 0. BRITT, TONY C. MOORE, AND CHARGES G. WADE. An Alternating Pulsed Magnetic Field Gradient Apparatus
for NMR
Self-Diffusion
. ZIMMERMANN.
Measurements
Quantitative
Spin Determination
by EPR Spectroscopy
G. M. MUHA. The Zeeman Effect in Spin = 1 Systems
,
JEN~ J. LED AND HENRIK GESMAR. The Applicability
of the MagnetizationTransfer NMR Technique to Determine Chemical Exchange Rates in Extreme Cases. The Importance of Complementary Experiments
J. 1. KAPLAN AND A. N. GARROWAY. Homogeneous
Distributions
and Inhomogeneous of Correlation Times. Lineshapes for Chemical Exchange
. BOSCAINO AND F. M. GELARDI. The Effect of the Spin Packet Lineshape
on the Saturation
of Inhomogeneous
Resonances
J. ISOYA, W. C. TENNANT, Y. UCHIDA, AND J. A. WEIL. Biradical
Center
in a-Quartz P. DIEHL, J. JOKISAARI, AND F. MOIA. Determination
of ‘H and i3C Chemical Shift Anisotropies. Comparison of Methods Using Acetonitrile as a Probe . .._.__..,_._.__,_._....._............_......._,.,_,
EDWARD P. DULIBA, EDMUND G. SEEBAUER, AND R. LINN BELFORD. Nu-
clear Quadrupole Coupling Cobalt(I1) System
in an EPR Investigation
of a Low-Spin 507
J. S. WAUGH. Systematic Procedure for Constructing coupling Sequences ___ ..,
Broadband
De517
LEV JACOBSON. Observation of Phosphorus-Phosphorus Dipolar Couplings by Two-Dimensional Nuclear Magnetization Exchange Spectroscopy . . . ... .. . . . . ...
522
T. C. NG, W. T. EVANOCHKO, AND J. D. GLICKSON. Faraday Shield for Surface Coil Studies of Subcutaneous Tumors
520
BURKHARDKIRSTEANDHANSVANWILLIGEN. tra of VO(acac)* in Frozen Solution
530
VLADIMIR MLYN~RIK. Indirect Coupling Constants AUTH~RINDEX
FORVOLUME~~
TripieResonanceSpec-
Measurement
of Nitrogen-Carbon 534
... . . . .
.
.
.
537
The Subject Index for Volume 49 will appear in the December 1982 issue as part of a cumulative index for the year 1982.
OF VOLUME
49
NUMBER 1, AUGUST 1982 C. V. LAGODZINSKAYA AND I. Yu. KLIMENKO. Measurement
tion for Magnetic Susceptibility with Solenoidal Magnet trometers .._._..._._._..._._..............._............._..
and CorrecNMR SpecE.
. J. OSTEN AND R. RADEGLIA. Spin Dynamics
of an AX System in FTNMR Experiment by the Example of the {‘H}-CW-Off-Resonance Decoupled r3C NMR Spectrum of Chloroform
JAMES F. HAW, T. E. GLASS, AND H. C. DORN. Conditions
Flow FT-‘H
NMR
Measurements
for Quantitative under Repetitive Pulse Conditions
8 22
DAVID T. PEGG, M. ROBIN BENDALL, AND DAVID M. DODDRELL. Ran-
domization
of Spins in Heteronuclear
Pulse Sequences
32
P. W. FRANCE AND M. WADSWORTH. Satellites and Shoulders in the NMR
“B Resonance of Borate Glass
48
KEIICHI OHNO. Application
of ESR Imaging to a Continuous Flow Method for Study on Kinetics of Short-Lived Radicals
J. N. HERAK, ALKA VELENIK, AND C. A. MCDOWELL. An ENDOR Study of Long-Range Spin Interactions in Molecular Crystals. II. The 5-Thymy1 Radical in a Single Crystal of Thymidine .. .. .. T. VAANANEN, J. JOKISAARI, AND J. LOUNILA. The Structure and Orientational Behavior of o&o-Difluorobenzene in Nematic Liquid Crystals
56
64 73
HENRY ZELDES AND RALPH LIVINGSTON. The Use of Spectral Simulations
for the Assay of Radical Concentrations R. C. BOWMAN, JR., AND W.-K.
for Second-Moment
by ESR
RHIM. A Simple Magic-Echo
84 Sequence
Measurements
93
P. DwBors MURPHY, T. TAKI, B. C. GERSTEIN, P. M. HENRICHS, AND D. J. MASSA. Shielding Anisotropies of 13C in Poly(ethylene terephthalate) . . ...__._..._....__.....__._.___....,.._.,__.,.,._ D. A. TORCIIIA AND ATTILA SZABO. Spin-Lattice
Relaxation
99
in Solids
P. J. HORE, M. R. EGMOND, H. T. EDZES, AND R. KAPTEIN. Cross-Re-
laxation Effects in the Photo-CIDNP Spectra of Amino Acids and Proteins . . .._......._.._.._...................._.._..._.._..
122
NOTES B. BL~MICH AND D. ZIESSOW. Skyline Projections in Two-Dimensional
NMR
Spectroscopy
P. N. TUTUNJIAN AND J. S. WAUGH. The Anisotropy
of the 31P-3iP
Indirect Nuclear Coupling G. HURST, K. KRAFT, R. SCHULTZ, AND R. KREILICK. Radiofrequency
Coil Construction
for a Bruker/IBM
ENDOR
Cavity
STEVEN L. PATT. Pulse Strategies for the Suppression of Acoustic Ring-
ing ..~.~.~....~~.~~~~~..~..~.....~~~~
., ._..
_. _.......
COMMUNICATIONS S. J. KARLIK, G. A. ELGAVISH, R. P. PILLAI, AND 6. L. EICHWORN.
Aluminum-27 NMR Studies of Al(III)-Phosphate Aqueous Solution .._ _........ __ . . . A. N. GARROWAY. Magic-Angle
Complexes in __ .._
Sample Spinning of Liquids
MICHAEL BATLEY AND JOHN W. REDMOND. 31PNMR
Reference Stan-
dards for Aqueous Samples DAVID L. TURNER. Carbon-13
Quantum
Coherence
Autocorrelation NMR Using Double~~.~~.~......~.~...~~~~~~..~.~.~_..~.
BOOK REVIEWS Ferromagnetodynamics: The Dynamics of Magnetic Bubbles, Domains and Domain Wails. T. H. O’Dell Specialist Periodical Reports. Spectroscopic Properties of Inorganic and Organometallic Compounds. D. M. Adams and E. A. V. Ebs-
worth, Senior Reporters Computer
Networks
in the Chemical
Laboratory.
Edited by George
C. Levy and Dan Terpstra NUMBER 2, SEPTEMBER 1982 DAVID M. DODDRELL, DAVID T. PEGG, AND M. ROIXN BENDALL.
stochastic J Cross-Polarization
in Liquids
.JOSEP~~ GRANOT. Resolution Effects in Spin-Lattice
surements
Relaxation Time
._..r.,,.._.___...._......__.........I._..........
THOMAS HERRLING, NORBERT KLIMES, WOLFGANG KARTHE, UWE EwERT, AND BERND EBERT. EPR Zeugmatography with Modulated ag-
netic Field Gradient PXOTR FAJER AND DEREK MARSH. Microwave
and Modulation Field homogeneities and the Effect of Cavity Q in Saturation Transfer E Spectra. Dependence on Sample Size
212
T. LIONEL, J. R. MORTON, AND K. F. PRESTON. The EPR Spectrum
of 225
Qs(CO)~+ Trapped in a Single Crystal of Cr(CO), W. SCHAJOR, U. HAEBERLEN, AND J. TEGENFELDT. Identification Characterization of the Motion of Water Molecules in Normal Deuterated Pyromellitic Acid Dihydrate
and and 233
The Interaction of Cobalt with Glycerophosphoryl Glycerol and Phosphatidyl Glycerol Bilayer Membranes
ALAN C. MCLAUGHLIN.
JOSEPH GRANOT. Paramagnetic
Relaxation
in Dipolar-Coupled
246
Homonu-
clear Spin Systems
251
T. C. NG, W. T. EVANOCHKO, R. N. HIRAMOTO, V. K. GHANTA, M. LILLY, A. J. LAWSON, T. H. CORBETT, J. R. DURANT, AND J. GLIcKSON. 31P NMR Spectroscopy of in Viva Tumors
271
B. B. SHARMA, G. CHIDICHIMO, A. SAUPE, H. CHANG, AND G. H. BROWN. Linewidth Analysis of the Proton Resonance Spectrum of Benzene in a Nematic Solution
287
W. WOLNEY FILHO, R. L. HAVILL, AND J. M. TITMAN. Nuclear elaxation in Molten Alkali Nitrates
2%
Spin
BRETT AND D. T. EDMONDS. 170 and ‘H NQR Study of Solid Meth-
anol Near Its Melting
Temperature
SOOK LEE, D. P. AMES, AND J. M. PUTNAM. Occurrence
of Abnormal Divergence Peaks in Axially Symmetric EPR Hyperhine Powder Spectra ..__....__.....__._...__..._._...._____._..__.___,,_._.
312
NOTES
9. HENNIG AND H. H. LIMBACH. Magnetization Transfer in the Rotating Frame: A New Simple Kinetic Tool for tbe Determination of Rate Constants in the Slow Chemical Exchange Range
322
NICHOLAS ZUMBULYADIS. Suppression of the Spinner Signal in Magic-
Angle-Spinning
NMR
A. LOEWENSTEIN. NMR
329 Study of the Azide Ion
332
ANTHONY S. SERIANNI AND ROBERT BARKER. 13C Spin-Lattice
laxation Times of [ l-‘3C]-Enriched
Re-
Carbohydrates
W. T. DIXON, JACOB SCHAEFER, M. D. SEFCIK, E. 0. STEJSKAL, AND R. A. MCKAY. Total Suppression of Sidebands in CPMAS C- 13 NMR ,.,......__..........___...__......._...___._.._. BRUCE COOK AND I. J. LOWE. A Large-Inductance,
High-Q, Series-Tuned Coil for NMR
335
341
High-Frequency, 346
COMMUNICATIONS A. SAMOSON, E. KUNDLA, AND E. LIPPMAA. High Resolution
NMR
of Quadrupolar
MAS-
Nuclei in Powders
ERHARD HAUPT. A Timesaving
Method to Determine the Length of a 90” Pulse ~~~...~~.~~.~~.~~~.~...~~~~........~.~~~...~~
T. TERAO, H. MIURA, AND A. SAIKA. Measurements of the 13C--lH Coupling Constants in Solid Adamantane: Resolution Enhancement by Multiple-Pulse Decoupling
365
P. DUBOIS MURPHY. Elimination of the Power Mismatch ments in Cross-Polarization NMR
368
Require-
NUMBER 3, OCTOBER ‘1, 1982 RONALD CROUCH, STUART HURLBERT, AND ARIS RAGOUZEOS. An Iter-
ative Linear Method for Calculation
of Spin-Lattice
Relaxation Times
CLAYDEN AND R. J. P. WILLIAMS. Peptide Group Shifts
371 383
Conformational Analysis of and Glycyl-L-Histidine from Nuclear-Nuclear . Spin Relaxation
BRUNT PERLY AND CLAUDE CHACHATY.
L-Alanyl-L-Tryptophan and Electron-Nuclear
397
MIRKO I. HROVAT, CHESTER 0. BRITT, TONY C. MOORE, AND CHARGES G. WADE. An Alternating Pulsed Magnetic Field Gradient Apparatus
for NMR
Self-Diffusion
. ZIMMERMANN.
Measurements
Quantitative
Spin Determination
by EPR Spectroscopy
G. M. MUHA. The Zeeman Effect in Spin = 1 Systems
,
JEN~ J. LED AND HENRIK GESMAR. The Applicability
of the MagnetizationTransfer NMR Technique to Determine Chemical Exchange Rates in Extreme Cases. The Importance of Complementary Experiments
J. 1. KAPLAN AND A. N. GARROWAY. Homogeneous
Distributions
and Inhomogeneous of Correlation Times. Lineshapes for Chemical Exchange
. BOSCAINO AND F. M. GELARDI. The Effect of the Spin Packet Lineshape
on the Saturation
of Inhomogeneous
Resonances
J. ISOYA, W. C. TENNANT, Y. UCHIDA, AND J. A. WEIL. Biradical
Center
in a-Quartz P. DIEHL, J. JOKISAARI, AND F. MOIA. Determination
of ‘H and i3C Chemical Shift Anisotropies. Comparison of Methods Using Acetonitrile as a Probe . .._.__..,_._.__,_._....._............_......._,.,_,
EDWARD P. DULIBA, EDMUND G. SEEBAUER, AND R. LINN BELFORD. Nu-
clear Quadrupole Coupling Cobalt(I1) System
in an EPR Investigation
of a Low-Spin 507
J. S. WAUGH. Systematic Procedure for Constructing coupling Sequences ___ ..,
Broadband
De517
LEV JACOBSON. Observation of Phosphorus-Phosphorus Dipolar Couplings by Two-Dimensional Nuclear Magnetization Exchange Spectroscopy . . . ... .. . . . . ...
522
T. C. NG, W. T. EVANOCHKO, AND J. D. GLICKSON. Faraday Shield for Surface Coil Studies of Subcutaneous Tumors
520
BURKHARDKIRSTEANDHANSVANWILLIGEN. tra of VO(acac)* in Frozen Solution
530
VLADIMIR MLYN~RIK. Indirect Coupling Constants AUTH~RINDEX
FORVOLUME~~
TripieResonanceSpec-
Measurement
of Nitrogen-Carbon 534
... . . . .
.
.
.
537
The Subject Index for Volume 49 will appear in the December 1982 issue as part of a cumulative index for the year 1982.