Atomic imaging of surfaces by electron microscopy

Atomic imaging of surfaces by electron microscopy

A658 462 Surface Science 178 (1986) 462-474 North-Holland, Amsterdam ATOMIC IMAGING OF SURFACES BY ELECTRON MICROSCOPY David J. SMITH Center for ...

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A658 462

Surface Science 178 (1986) 462-474 North-Holland, Amsterdam

ATOMIC IMAGING OF SURFACES

BY ELECTRON

MICROSCOPY

David J. SMITH Center for Solid State Science and Department of Physics, Arizona State (/niuersi!y, Tempe, AZ 85287, USA Received

25 April 1986; accepted

for publication

18 June 1986

Electron microscopes with atomic resolution have recently been used to study surfaces and to observe surface processes in real-time. The role of image simulations in confirming the interpretation of surface profile images is discussed and recent applications of the profile imaging technique to study semiconductors, oxides, the oxidation of metals, and small metal particles are briefly reviewed. Finally, the accumulation of metal deposits on some oxide and semiconductor surfaces due to electron-stimulated desorption processes is described.

475

Surface Science 178 (1986) 475-482 North-Holland, Amsterdam

LOW ENERGY ION SCA’ITERING J. MijLLER,

K.J. SNOWDON

FROM THE Au(ll0)

SURFACE

*, W. HEILAND

Fachbereich Physik, Universitiii Osnabriick, P.O. Box 4469, D-4500 Osnabriick, Fed. Rep. of Germany

and H. NIEHUS Institul fiir Grenzfliichenforschung und Vakuumphysik der KFA Jiilich, P.O. Box 1913, D-51 70 Jiilich, Fed. Rep. of Germany Received

14 March

1986; accepted

for publication

30 April 1986

The location of the outermost atomic layer relative to the second one of the reconstructed clean Au(llO)-(1 x 2) surface has been directly determined by large angle (165O) low energy (2000 ev) Ne+,Ne’ backscattering. The surface forms the expected “missing row” structure with a 0.20&0.07 A contraction of the first layer relative to the bulk determined atomic positions. Temperature dependent measurements (300 < T< 800 K) have been performed at a scattering angle of 123O using Na+ in order to follow the phase transition from the (1 X 2) to the (1 x 1) structure. The ion scattering data measured in the (112) azimuth show a pronounced decrease of the characteristic slopes for the (1 X 2) structure and an increase of signals related with the (1 X 1) structure upon temperature increase above 700 K. We also find evidence for the existence of monoatomic steps coexisting with both structures.