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Contents of volume 72
CONTENTS
OF VOLUME
72
NUMBER 1, MARCH 1987 YUIUO HIYAMA, PETER M. WOYCIESJES,THEODORE L. BROWN, AND DENNIS A. TORCHIA. Magnesium-25 Nuclear Quadrupole Resonance . . . . . .
1
D. L. VANDERHART. Natural-Abundance i3C-r3C Spin Exchange in Rigid Crystalline Organic Solids . . ..... .... .... .. .
13
J. C. MACDONALD AND M. MAZUREK. Phosphorus Magnetic Spectra of Open-Chain Linear Polyphosphates . . ...
Resonance ..
48
G. J. BOWDEN AND W. D. HUTCHISON. Tensor Operator Formalism for Multiple-Quantum NMR. 4. Spin-s Nuclei with an Asymmetry Term in the Quadrupole Hamiltonian .. ... . . . ..
61
ANNJIA T. Hsu, WILLIAM W. HUNTER, JR., PETRA SCHMALBROCK, AND ALAN G. MARSHALL. Stored Waveform Inverse Fourier-Transform (SWIFT) Excitation for Water-Suppressed Whole-Body Slice-Selected Proton Chemical Shift Spectra at 1.5 Tesla . ... . .
75
M. S. GREENFIELD, A. D. RONEMUS, R. L. VOLD, R. R. VOLD, P. D. ELLIS, AND T. E. RAIDY. Deuterium Quadrupole-Echo NMR Spectroscopy. III. Practical Aspects of Lineshape Calculations for Multiaxis Rotational Processes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
89
R. A. WIND AND C. S. YANNONI. ‘H-13C Polarization Transfer via the Nuclear SolidEffect . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
108
SARAH L. HEALD, LUCIANO MUELLER, AND PETER W. JEFFS. Structural Analysis of Teicoplanin A2 by 2D NMR . . . .. . ..
120
JUDY P. LEE AND MELVIN B. COMISAROW. The Phase Dependence of MagnitudeSpectra . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . .. . . . . . .
139
MICHAEL MURPHY, MYRON G. SEMACK, AND DAVID WHITE. Zeeman and Dipolar Coherences in Dilute Spin Z = 1 Powders. Matrix-Isolated CH3CN
143
NOTES JAMES PEKAR, PERRY F. RENSHAW, AND JOHN S. LEIGH, JR. Selective Detection of Intracellular Sodium by Coherence-Transfer NMR .
159
ROBERT W. DYKSTRA. Elimination of the Inhomogeneous Part of a Solvent Signal Improves the Spectra of Millimolar Solutes . . . . . .
162
L.-H. CHANG, W. M. CHEW, P. R. WEINSTEIN, AND T. L. JAMES. A Balanced-Matched Double-Tuned Probe for in Viva ‘H and 31PNMR
168
COMMUNICATIONS KEITH R. CARDUNER. A Method for the Implementation of Protonated Carbon Suppression with the Total Suppression of Spinning Sidebands (TOSS) . .. .. . ... .. .. . .
173
EMIL UGURBIL, MICHAEL GARWOOD, AND M. ROBIN BENDALL. Amplitude- and Frequency-Modulated Pulses to Achieve 90” Plane Rotations with Inhomogeneous B, Fields .. ..
177
M. J. BOGUSKY, R. A. SCHIKSNIS, G. C. LEO, AND S. J. OPELLA. Protein Backbone Dynamics by Solid-State and Solution 15N NMR Spectroscopy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
186
LUCIANO MUELLER. P.E.COSY, a Simple Alternative to E.COSY
191
B. T. FARMER II AND L. R. BROWN. The Effect of Resonance Offset on the Cross-Relaxation Rate in the Rotating Frame . .
197
STEVEN R. MAPLE AND ADAM ALLERHAND. Analysis of Minor Components by Ultrahigh Resolution NMR. I. Evidence for the Detectability of Weak Resonances near Peaks Which Are 10,000 Times Larger, without Suppression of the Large Peaks . .
203
NUMBER~,APRIL
1987
P. MANSFIELD AND B. CHAPMAN. Multishield Active Magnetic Screening of Coil Structures in NMR . . .. . .. . . .. ,.
211
P.J. McD~NALD,J.J. ATTARD, AND D. G. TAYLOR. A New Approach to the NMR Imaging of Solids . . . .. .. ,
224
S. R. RABBANI, D. T. EDMONDS, P. GOSLING, AND M. H. PALMER. Measurement of the 14N Quadrupole Coupling Constants in Glycine, Diglycine, Triglycine, and Tetraglycine and a Comparison with Calculation ..
230
DANIELP. RALEIGH,EDWARD T.~LEJNICZAK, SHIMONVEGA,ANDROBERT G. GRIFFIN. An Analysis of Sideband Suppression Techniques in MagicAngle Sample Spinning NMR . . .. . . . .
238
Y. AYANT, A. THEVAND, L. WERBELOW, AND P. TORDO. Determination of the Absolute Sign of the I70 Isotropic Hyperfine Coupling Constant in the Diarylphosphonyl Radical, (2,4,6-But3CsH2)&‘=0 .. .. . . .
251
MARTIND.KING,JORG-HEINOSACHSE,ANDDEREK M~~~~.Unconstrained Optimization Method for Interpreting the Concentration and Temperature Dependence of the Linewidths of Interacting Nitroxide Spin Labels. Application to the Measurement of Translational Diffusion Coefficients of Spin-Labeled Phospholipids in Membranes . . . . . . .
257
P. GOSLING, D. T. EDMONDS, AND S. R. RABBANI. A Zero-Field NQR and Low-Field NMR Study of NaHFz and RI-IF, . ..... ... .
268
MUNEKI OHUCHI, MASAMI HOSONO, KAZUO FURIHATA, AND HARUO SETO. A Method for Pure Absorption 2D Spectroscopy Using Complex Fourier Transformation in Both Dimensions . ... . ... . ....
279
SCOTT M. ELEFF, V. HARIHARA SUBRAMANIAN, MEIR SHINNAR, SCOT RENN, AND JOHN S. LEIGH, JR. The Synthesis of Pulse Sequences Yielding Arbitrary Symmetric Magnetization Vectors . . . .. . . ..
298
JENS FRAHM, WOLFGANG H,&NICKE, AND KLAUS-DIETMAR Transverse Coherence in Rapid FLASH NMR Imaging
307
MERBOLDT. .
T. TSANG, R. M. FRONKO, AND H. A. RESING. Indirect Measurement of 14N Quadrupolar Coupling for NH3 Intercalated in Potassium Graphite . .
315
NOTES MICHAEL A. WEISS AND JEFFREY C. HOCH. Interpretation of Ring-Current Shifts in Proteins: Application to Phage X Repressor . .
324
D. G. CORY AND W. M. RITCHEY. A Simple Pulsed Amplifier Controller
334
ROGER H. NEWMAN. Effects of Finite Preparation-Pulse Power on Carbon13 Cross-Polarization NMR Spectra of Heterogeneous Samples
337
YOSHITERU SEO, MASATAKA MURAKAMI, TAKEHISA MATSUMOTO, HIROYASU NISHIKAWA, AND HIROSHI WATARI. Applications of Aqueous Shift Reagent, Dy(TTHA), for 23Na NMR Studies of Exocrine Glands. Viabilities of Organs Perfused with Shift Reagent
341
B. T. FARMER II, S. MACURA, AND L. R. BROWN. Relay Artifacts in ROESY Spectra . . ... . .... . .. . ... .
347
B. M. FUNG. A Comparison of Homonuclear niques in Heteronuclear Experiments
Dipolar-Decoupling Tech.. . .
353
WALTER J. CHAZIN AND KURT WUTHRICH. Optimization of Homonuclear Relayed Coherence Transfer Experiments with Proteins in Hz0 Solution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
358
BARNEY L. BALES, KIMBERLY L. SCHUMACHER, AND FRANCIS L. HARRIS. Correction for Inhomogeneous Line Broadening in Spin Labels. III. Doxyl-Labeled Alkyl Chains’ . . .. . . .. . .
364
MICHAEL P. WILLIAMSON AND DAVID NEUHAUS. Symmetry in NOE Spectra . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
369
ROBERT G. BRYANT, SUBRAMANIAN GANAPATHY, AND SCOTT D. KENNEDY. High-Resolution Calcium-43 NMR in Solids . ..
376
COMMUNICATIONS R. KIMMICH AND D. HOEPFEL. Volume-Selective Multipulse Spin-Echo Spectroscopy ............................................
379
ROBIN K. HARRIS, KENNETH J. PACKER, PATRICK ANGELIKA SEBALD. High-Resolution Tin-l 19 NMR methyltin Hydroxide. Erratum and Further Comment
REAMS, AND of Solid Tri..
385
M. ROBERTS, AND WAYNE T. FERNMR of Abundant Spins in Solids
388
LEWIS E. KAY, PAUL-JAMES JONES, AND J. H. PRESTEGARD. Strong Coupling Effects in the Homonuclear RELAY Experiment, with Applications to Leucine Spin Systems of Octanoyl-Acyl Carrier Protein
392
NICHOLAS ZUMBULYADIS, PAMELA RAR. Two-Dimensional
MAS
NUMBER T. E. BULL.
Cross-Correlation
3, MAY
and 2D NOE
1987
Spectra
.
...
397
TAITO VUNANEN, JUKKA JOKISAARI, AND MAARIA SELANTAUS. A VariableAngle Spinning System for the Determination of NMR Parameters of Liquid-Crystalline Samples . .. .. .. . .. . .
414
S. R. RABBANI, D. T. EDMONDS, AND P. GOSLING. Nuclear Quadrupole Resonance of 14N and ‘H in Pyrimidines, Purities, and Their Nucleosides
422
A. KELLER, SONJA BENZ, AND U. HAEBERLEN. NMR Lineshape Analysis Exchanging Systems. Mapping onto Harmonic Oscillator Equations; New Analytically Solvable Case and Experiments on K&O2 * D20
434
MARTIN M. MALTEMPO, SANDRA tral-spatial Two-Dimensional S. MULLER
of A
S. EATON, AND GARETH R. EATON. SpecEPR Imaging . ... .. ..
AND J. SEELIG. In I’ivo NMR
.
456
on .
467
Effects .. ..
475
ERNEST D. LAUE, KONRAD 0. B. POLLARD, JOHN SKILLING, JAMES STAUNTON, AND ANDREW C. SUTKOWSKI. Use of the Maximum Entropy Method to Correct for Acoustic Ringing and Pulse Breakthrough in 170 NMRSpectra ...............................................
493
JENS FRAHM, KLAUS-DIETMAR calized Proton Spectroscopy
HANICKE. Lo... ... .
502
ANDREW HASENFELD. A Connection between the Bloch Equations and the Korteweg-de Vries Equation .. .... .. . .. .. . .
509
MAZIAR SARDASHTI Cross Polarization
Imaging
AND GARY E. MACIEL. . . . ....
PETER PF~~NDLER AND GEOFFREY in z-Filtered Two-Dimensional
of Deuterium
Effects ..
BODENHAUSEN. NMR Correlation
.
449
of Sample Spinning .. .... .. .. Strong Coupling Spectra
MERBOLDT, AND WOLFGANG Using Stimulated Echoes
P.-O. WESTLUND AND R. M. LYNDEN-BELL. A Molecular Dynamics Study of the Intermolecular Spin-Spin Dipole-Dipole Correlation Function of Liquid Acetonitrile . .. . . ... . .. .
522
D. M. LAMB,P.J.GRANDINETTI, AND J. JONAS. Fixed Field Gradient NMR Diffusion Measurements Using Bessel Function Fits to the Spin-Echo Signal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
532
NOTES A. A. BOTHNER-BY AND J. DADOK. Useful Manipulations of the Free Induction Decay . ... . ... .. . ..
540
CARIN STADER AND BERND WRACKMEYER. Natural Abundance “N Nuclear Magnetic Resonance of Monomeric Cyclic and Noncyclic Tin(I1) and Lead(I1) Amides .. .. . . .
544
P. KUHNS,O.GONEN,ANDJ. at Low Temperatures
W~u~~.NMRLineshape Thermometry ... . . .
548
YISHAY MANASSEN, GIL NAVON, AND C. T. W. MOONEN. Reduced Multidimensional NMR Experiments Using a Linear Least-Squares Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
551
ANDREW S. ZEKTZER, BOBAN K. JOHN, RAYMOND N. CASTLE, AND GARY E. MARTIN. “Decoupling” Modulations Due to One-Bond Heteronuclear Spin Couplings in Long-Range Heteronuclear Chemical-shift Correlation Spectra . . .
556
R. 0. DAY, J. L. RAGLE, AND Y. YOSHIDA. Deuteron Quadrupole Coupling at C8 in Adenosine, Inosine, and Guanosine Dihydrate at 77K . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .._....
562
A. M. THAYER, M. LUZAR, AND A. PINES. Heteronuclear .. . .. NMR of Liquid Crystals . .
567
COMMUNICATIONS
Zero-Field
JOHNM.BEALE,CHARLESE.COTTRELL,PAUL J. KELLER,ANDHEINZ G. FLOSS. Development of Triple-Quantum “INADEQUATE” for Biosynthetic Studies . . ... . . .
574
L. BRAUNSCHWEILER,A.SCHWEIGER,J.M.FAUTH,ANDR.R.ERNST. Determination of the Microwave Field Strength by Microwave-Induced Transitory Oscillations in Pulsed Electron Spin Resonance
579
Z. MADI, B. U. MEIER, AND R. R. ERNST. Detection of Cross Peaks in Two-Dimensional NMR by Cluster Analysis . . .. .
584
MEETINGSANDANNOUNCEMENTS AUTHORINDEXFORVOLUME72
. . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . .
591
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . .
592
The Subject Index for Volume 72 will appear in the December 1987 issue as part of a cumulative index for the year 1987.
OF VOLUME
72
NUMBER 1, MARCH 1987 YUIUO HIYAMA, PETER M. WOYCIESJES,THEODORE L. BROWN, AND DENNIS A. TORCHIA. Magnesium-25 Nuclear Quadrupole Resonance . . . . . .
1
D. L. VANDERHART. Natural-Abundance i3C-r3C Spin Exchange in Rigid Crystalline Organic Solids . . ..... .... .... .. .
13
J. C. MACDONALD AND M. MAZUREK. Phosphorus Magnetic Spectra of Open-Chain Linear Polyphosphates . . ...
Resonance ..
48
G. J. BOWDEN AND W. D. HUTCHISON. Tensor Operator Formalism for Multiple-Quantum NMR. 4. Spin-s Nuclei with an Asymmetry Term in the Quadrupole Hamiltonian .. ... . . . ..
61
ANNJIA T. Hsu, WILLIAM W. HUNTER, JR., PETRA SCHMALBROCK, AND ALAN G. MARSHALL. Stored Waveform Inverse Fourier-Transform (SWIFT) Excitation for Water-Suppressed Whole-Body Slice-Selected Proton Chemical Shift Spectra at 1.5 Tesla . ... . .
75
M. S. GREENFIELD, A. D. RONEMUS, R. L. VOLD, R. R. VOLD, P. D. ELLIS, AND T. E. RAIDY. Deuterium Quadrupole-Echo NMR Spectroscopy. III. Practical Aspects of Lineshape Calculations for Multiaxis Rotational Processes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
89
R. A. WIND AND C. S. YANNONI. ‘H-13C Polarization Transfer via the Nuclear SolidEffect . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
108
SARAH L. HEALD, LUCIANO MUELLER, AND PETER W. JEFFS. Structural Analysis of Teicoplanin A2 by 2D NMR . . . .. . ..
120
JUDY P. LEE AND MELVIN B. COMISAROW. The Phase Dependence of MagnitudeSpectra . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . .. . . . . . .
139
MICHAEL MURPHY, MYRON G. SEMACK, AND DAVID WHITE. Zeeman and Dipolar Coherences in Dilute Spin Z = 1 Powders. Matrix-Isolated CH3CN
143
NOTES JAMES PEKAR, PERRY F. RENSHAW, AND JOHN S. LEIGH, JR. Selective Detection of Intracellular Sodium by Coherence-Transfer NMR .
159
ROBERT W. DYKSTRA. Elimination of the Inhomogeneous Part of a Solvent Signal Improves the Spectra of Millimolar Solutes . . . . . .
162
L.-H. CHANG, W. M. CHEW, P. R. WEINSTEIN, AND T. L. JAMES. A Balanced-Matched Double-Tuned Probe for in Viva ‘H and 31PNMR
168
COMMUNICATIONS KEITH R. CARDUNER. A Method for the Implementation of Protonated Carbon Suppression with the Total Suppression of Spinning Sidebands (TOSS) . .. .. . ... .. .. . .
173
EMIL UGURBIL, MICHAEL GARWOOD, AND M. ROBIN BENDALL. Amplitude- and Frequency-Modulated Pulses to Achieve 90” Plane Rotations with Inhomogeneous B, Fields .. ..
177
M. J. BOGUSKY, R. A. SCHIKSNIS, G. C. LEO, AND S. J. OPELLA. Protein Backbone Dynamics by Solid-State and Solution 15N NMR Spectroscopy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
186
LUCIANO MUELLER. P.E.COSY, a Simple Alternative to E.COSY
191
B. T. FARMER II AND L. R. BROWN. The Effect of Resonance Offset on the Cross-Relaxation Rate in the Rotating Frame . .
197
STEVEN R. MAPLE AND ADAM ALLERHAND. Analysis of Minor Components by Ultrahigh Resolution NMR. I. Evidence for the Detectability of Weak Resonances near Peaks Which Are 10,000 Times Larger, without Suppression of the Large Peaks . .
203
NUMBER~,APRIL
1987
P. MANSFIELD AND B. CHAPMAN. Multishield Active Magnetic Screening of Coil Structures in NMR . . .. . .. . . .. ,.
211
P.J. McD~NALD,J.J. ATTARD, AND D. G. TAYLOR. A New Approach to the NMR Imaging of Solids . . . .. .. ,
224
S. R. RABBANI, D. T. EDMONDS, P. GOSLING, AND M. H. PALMER. Measurement of the 14N Quadrupole Coupling Constants in Glycine, Diglycine, Triglycine, and Tetraglycine and a Comparison with Calculation ..
230
DANIELP. RALEIGH,EDWARD T.~LEJNICZAK, SHIMONVEGA,ANDROBERT G. GRIFFIN. An Analysis of Sideband Suppression Techniques in MagicAngle Sample Spinning NMR . . .. . . . .
238
Y. AYANT, A. THEVAND, L. WERBELOW, AND P. TORDO. Determination of the Absolute Sign of the I70 Isotropic Hyperfine Coupling Constant in the Diarylphosphonyl Radical, (2,4,6-But3CsH2)&‘=0 .. .. . . .
251
MARTIND.KING,JORG-HEINOSACHSE,ANDDEREK M~~~~.Unconstrained Optimization Method for Interpreting the Concentration and Temperature Dependence of the Linewidths of Interacting Nitroxide Spin Labels. Application to the Measurement of Translational Diffusion Coefficients of Spin-Labeled Phospholipids in Membranes . . . . . . .
257
P. GOSLING, D. T. EDMONDS, AND S. R. RABBANI. A Zero-Field NQR and Low-Field NMR Study of NaHFz and RI-IF, . ..... ... .
268
MUNEKI OHUCHI, MASAMI HOSONO, KAZUO FURIHATA, AND HARUO SETO. A Method for Pure Absorption 2D Spectroscopy Using Complex Fourier Transformation in Both Dimensions . ... . ... . ....
279
SCOTT M. ELEFF, V. HARIHARA SUBRAMANIAN, MEIR SHINNAR, SCOT RENN, AND JOHN S. LEIGH, JR. The Synthesis of Pulse Sequences Yielding Arbitrary Symmetric Magnetization Vectors . . . .. . . ..
298
JENS FRAHM, WOLFGANG H,&NICKE, AND KLAUS-DIETMAR Transverse Coherence in Rapid FLASH NMR Imaging
307
MERBOLDT. .
T. TSANG, R. M. FRONKO, AND H. A. RESING. Indirect Measurement of 14N Quadrupolar Coupling for NH3 Intercalated in Potassium Graphite . .
315
NOTES MICHAEL A. WEISS AND JEFFREY C. HOCH. Interpretation of Ring-Current Shifts in Proteins: Application to Phage X Repressor . .
324
D. G. CORY AND W. M. RITCHEY. A Simple Pulsed Amplifier Controller
334
ROGER H. NEWMAN. Effects of Finite Preparation-Pulse Power on Carbon13 Cross-Polarization NMR Spectra of Heterogeneous Samples
337
YOSHITERU SEO, MASATAKA MURAKAMI, TAKEHISA MATSUMOTO, HIROYASU NISHIKAWA, AND HIROSHI WATARI. Applications of Aqueous Shift Reagent, Dy(TTHA), for 23Na NMR Studies of Exocrine Glands. Viabilities of Organs Perfused with Shift Reagent
341
B. T. FARMER II, S. MACURA, AND L. R. BROWN. Relay Artifacts in ROESY Spectra . . ... . .... . .. . ... .
347
B. M. FUNG. A Comparison of Homonuclear niques in Heteronuclear Experiments
Dipolar-Decoupling Tech.. . .
353
WALTER J. CHAZIN AND KURT WUTHRICH. Optimization of Homonuclear Relayed Coherence Transfer Experiments with Proteins in Hz0 Solution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
358
BARNEY L. BALES, KIMBERLY L. SCHUMACHER, AND FRANCIS L. HARRIS. Correction for Inhomogeneous Line Broadening in Spin Labels. III. Doxyl-Labeled Alkyl Chains’ . . .. . . .. . .
364
MICHAEL P. WILLIAMSON AND DAVID NEUHAUS. Symmetry in NOE Spectra . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
369
ROBERT G. BRYANT, SUBRAMANIAN GANAPATHY, AND SCOTT D. KENNEDY. High-Resolution Calcium-43 NMR in Solids . ..
376
COMMUNICATIONS R. KIMMICH AND D. HOEPFEL. Volume-Selective Multipulse Spin-Echo Spectroscopy ............................................
379
ROBIN K. HARRIS, KENNETH J. PACKER, PATRICK ANGELIKA SEBALD. High-Resolution Tin-l 19 NMR methyltin Hydroxide. Erratum and Further Comment
REAMS, AND of Solid Tri..
385
M. ROBERTS, AND WAYNE T. FERNMR of Abundant Spins in Solids
388
LEWIS E. KAY, PAUL-JAMES JONES, AND J. H. PRESTEGARD. Strong Coupling Effects in the Homonuclear RELAY Experiment, with Applications to Leucine Spin Systems of Octanoyl-Acyl Carrier Protein
392
NICHOLAS ZUMBULYADIS, PAMELA RAR. Two-Dimensional
MAS
NUMBER T. E. BULL.
Cross-Correlation
3, MAY
and 2D NOE
1987
Spectra
.
...
397
TAITO VUNANEN, JUKKA JOKISAARI, AND MAARIA SELANTAUS. A VariableAngle Spinning System for the Determination of NMR Parameters of Liquid-Crystalline Samples . .. .. .. . .. . .
414
S. R. RABBANI, D. T. EDMONDS, AND P. GOSLING. Nuclear Quadrupole Resonance of 14N and ‘H in Pyrimidines, Purities, and Their Nucleosides
422
A. KELLER, SONJA BENZ, AND U. HAEBERLEN. NMR Lineshape Analysis Exchanging Systems. Mapping onto Harmonic Oscillator Equations; New Analytically Solvable Case and Experiments on K&O2 * D20
434
MARTIN M. MALTEMPO, SANDRA tral-spatial Two-Dimensional S. MULLER
of A
S. EATON, AND GARETH R. EATON. SpecEPR Imaging . ... .. ..
AND J. SEELIG. In I’ivo NMR
.
456
on .
467
Effects .. ..
475
ERNEST D. LAUE, KONRAD 0. B. POLLARD, JOHN SKILLING, JAMES STAUNTON, AND ANDREW C. SUTKOWSKI. Use of the Maximum Entropy Method to Correct for Acoustic Ringing and Pulse Breakthrough in 170 NMRSpectra ...............................................
493
JENS FRAHM, KLAUS-DIETMAR calized Proton Spectroscopy
HANICKE. Lo... ... .
502
ANDREW HASENFELD. A Connection between the Bloch Equations and the Korteweg-de Vries Equation .. .... .. . .. .. . .
509
MAZIAR SARDASHTI Cross Polarization
Imaging
AND GARY E. MACIEL. . . . ....
PETER PF~~NDLER AND GEOFFREY in z-Filtered Two-Dimensional
of Deuterium
Effects ..
BODENHAUSEN. NMR Correlation
.
449
of Sample Spinning .. .... .. .. Strong Coupling Spectra
MERBOLDT, AND WOLFGANG Using Stimulated Echoes
P.-O. WESTLUND AND R. M. LYNDEN-BELL. A Molecular Dynamics Study of the Intermolecular Spin-Spin Dipole-Dipole Correlation Function of Liquid Acetonitrile . .. . . ... . .. .
522
D. M. LAMB,P.J.GRANDINETTI, AND J. JONAS. Fixed Field Gradient NMR Diffusion Measurements Using Bessel Function Fits to the Spin-Echo Signal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
532
NOTES A. A. BOTHNER-BY AND J. DADOK. Useful Manipulations of the Free Induction Decay . ... . ... .. . ..
540
CARIN STADER AND BERND WRACKMEYER. Natural Abundance “N Nuclear Magnetic Resonance of Monomeric Cyclic and Noncyclic Tin(I1) and Lead(I1) Amides .. .. . . .
544
P. KUHNS,O.GONEN,ANDJ. at Low Temperatures
W~u~~.NMRLineshape Thermometry ... . . .
548
YISHAY MANASSEN, GIL NAVON, AND C. T. W. MOONEN. Reduced Multidimensional NMR Experiments Using a Linear Least-Squares Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
551
ANDREW S. ZEKTZER, BOBAN K. JOHN, RAYMOND N. CASTLE, AND GARY E. MARTIN. “Decoupling” Modulations Due to One-Bond Heteronuclear Spin Couplings in Long-Range Heteronuclear Chemical-shift Correlation Spectra . . .
556
R. 0. DAY, J. L. RAGLE, AND Y. YOSHIDA. Deuteron Quadrupole Coupling at C8 in Adenosine, Inosine, and Guanosine Dihydrate at 77K . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .._....
562
A. M. THAYER, M. LUZAR, AND A. PINES. Heteronuclear .. . .. NMR of Liquid Crystals . .
567
COMMUNICATIONS
Zero-Field
JOHNM.BEALE,CHARLESE.COTTRELL,PAUL J. KELLER,ANDHEINZ G. FLOSS. Development of Triple-Quantum “INADEQUATE” for Biosynthetic Studies . . ... . . .
574
L. BRAUNSCHWEILER,A.SCHWEIGER,J.M.FAUTH,ANDR.R.ERNST. Determination of the Microwave Field Strength by Microwave-Induced Transitory Oscillations in Pulsed Electron Spin Resonance
579
Z. MADI, B. U. MEIER, AND R. R. ERNST. Detection of Cross Peaks in Two-Dimensional NMR by Cluster Analysis . . .. .
584
MEETINGSANDANNOUNCEMENTS AUTHORINDEXFORVOLUME72
. . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . .
591
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . .
592
The Subject Index for Volume 72 will appear in the December 1987 issue as part of a cumulative index for the year 1987.