- Email: [email protected]
Fabrication of a Novel Nano-engineered Glass Based Optical Fiber for Radiation Sensor Application
Available online at www.sciencedirect.com
ScienceDirect Procedia Materials Science 10 (2015) 683 – 692
) *(+ ! , *+ -
!"#
!"#$$% &' & ()))*+ , - $ $
! ( $ (
( # * *"# ! # ! ! ,
$ ($ !#,! ( ! # *./
# ! # , !0# , ! #%( ! $! # 1* , # 12 , ! !
%($ !* *"# ($ (# $-1-234% -2134%5 % ! 6 # ! ! * *"# ($ ! , 6 #!! $# (# (($ $ % $ © 2015 The!"# ! #$ !$%& ' Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). # $ %( !) *(+ ! , *+ - Peer-review under responsibility of the International Conference on Nanomaterials and Technologies (CNT 2014) './
7 ($5* "# ,
5,, 5/( 5)#
58
$ !
7 ($$ , ! !,! % #! # 5! 9 # ) ( !( ( , ! % ( (# ( ! 7 ($ $, % , % ( % $ (( !% (( ,
($ 5 # $ $ 6 ( # : ;# / % $$ !( ( #( , ,
: # < 4! ! 5 ! ( , ( 6 , 5 # $% ! % % # # ' 7' = <<25 8% <<> " ! % # ! (
!
# ( # ( ($ ($ % %
?* , # ! @A< 22 - 2 2:( 6@A< 22 ->2<> 0
1 , - $ $
2211-8128 © 2015 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). Peer-review under responsibility of the International Conference on Nanomaterials and Technologies (CNT 2014) doi:10.1016/j.mspro.2015.06.068
684
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
$ ( %5 % ! " 5#! ! ( % ($ ! ( # $ ! % ! %( $ ($ ! ((( #! 45 " 5 % :4! ! 5 = <<25 # <5 B$ < 4 # ($ !#! % ! ! (" ($ : # < ($ $ , ( # !#,! % %!,! 7# # %!,! ($ ! ! ( ($ 5!! $%(( (# % % # , ! ,! #C# D ; + ( , !12 ) ! ! * "# , # ! ! ,
$
% ($ $ !( ,( $# ! (* "# ,
*"# ,
! 6 ! ((%(,% (( !! ,
6 !
B# !5 * ,
! # ( ! !# !$ $ ! *7
,, 6 ( *2A *-A : * #! ( # ! ! ,
!* *"# !# %( ($ $ ) ! 5 ! # (* ($ ( % !#,! # (#
#$%(( D ( #%
! # ( !
! (* *"# , # ! ! ,
$ ($ !#,! ! ( *! . / *./ !0## ! # ,
, ! #%( ! $! ## 1* , # ! ! 9 # ( ! , ! (* *"# , ,
!#,! & 5 & &/E $ ! ,, (( ( * 5 ( ( # ! $! ( ($ # ! ( F % , ! #
! &8 #% ! $ ( , ($ ! $ ( ! ! (* ! # ! ! ,
$ ($ ! !,! %5, % ! ! ## % ( ,$! #6!$ , %! *"# ($ ! % ! , , % ! ! ## $! 5 #,, , %
&' (
(
! *./
# ! ! # , !0#! $# ( $ % ( ,,
$ ($ ( !
( ! # % , 7 !7 G* ! # , % 0# 9 #$# B 2, (# - ! #$ !D
( ! # % !#,! )8 % 87 -- * B7. 3 " -*5H * 5 I" ! # # %(G* %!# % ! !6% !%,$# 9 ! % ( ! % ! # % 6 ( ! ,
D, ! , 0## # , # $ ! ( (( " 5* "#((6 (-# B (* ( 5 # # $
, ! ( " * 2 1;7 ** 2 >;7 5 ! ( *"# 0# # ( " * 2 1;75 ** 2 >;7 "#* 2
! ( ## # % ! # , ( ! ! 8& : +,#% >5 ) ! < >5 $ ! ,8& # # #(8& ) 5 ! " ! (* , :" < 1 ! #$ ! D % ! # ,
D, ! ( $% !% 6 $% , ! # ( < >* B %5 ! #$! $ % ! ! ( !($ ( GJ! $ ( !( $ ( ! ! 5 # 5 ((
685
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
C# #! ! ! ! ! ! ( ! ! ( ! $ !( $ ! ! ! ( #$ ! # %: # < ! ( ! * *"# ($ ( $ $ /
@/ (( $ * / - *"# / ($
0
/ - /
(
1(.
7A7 *7A" 72
7A7 A*7A"#72A" 72
1
$ !
2
( ! (
& 3
!+
!6 # # # ! $! (*/ - *"#/ # ! ! ,
$ ($ $ : # <"$# , ! (($ # ( ! ( ! ( ! $% ! ,, ! $ ! ($ ! 1* , # # ! (( ( !($ ! $% %, !6 # ((( ! ,! # 0# 9H! , 5 ,! $ % GK ! ! ,! ,# ( !($ ! !- , ! ,5 # #6 ! 1* , # D ! ,% . # ! #
, ! % % # !(( #! 5 8 ! 12 ! ! ##
! 4%
4
! #( ! ,%( ( / - / !(( * "# 6 # , , & & ! ! ( ! ( $ ($ & , 8 &8 $ ($ E $ &8 D@ 3#D 3 @ "2 ( ! (8 ! $ #&/E % ((/ - / # ! ! ( B, , ! (* "# ! , , ( (( # ! ( ! ( (# $# K " 725 K 75 2 K *7 / - ($ ! ! , , ! / # K " 725 K 75 > K *75 K "#72 3 ! ! ($ # ,# # (# ( " ( # " L1 K " 72($( $ *)8 *4*8) # !6 ( ! % %
%% %%
*% *% )% )% "% "% % % % % % " ) * % " % " ) * % " & +,- . & +,- .
&/E ( (* *"# $($ (
B, ! ( ! ( ( $ ! ! ($ #
686
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
687
688
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
689
690
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
691
692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
,
# !,! % ! #( (8 ! 8 ! !!,! %(* ($ -1-234% ! ! (*"# ($ -2134% ! % % ! # 12 " ! # ! ! ($ #! # $ ( ! ! ($
; < (
"# ! ! D ,/8/7 +/ !(( # ! # ! ! D(# ! O / ,# 5 / *)8 *4*8)(! ## # , 5,# # ! D
3
" 5O5+ D 5;5O# 5O ; 5 5< 15" ## ! !# ,(( !( # # # (%# ,
5=# (" !% <52-2 2-21
"$ , 5" 3 %535<>5& , 8 ( ) 576(5* 3 %53 5OH;5<25 , 58 ,!% 15 <
* 5*5 5 5 995B5 585* #5 5 # #5"5O 585 9955 ,!5"53 5 55 $ %( # # ! ,
($%$ ! !# 5=# (" *! % >5-1 -1<
B$ 5&=5!# 95*54,!5 &5< 5* (( ! (4 ($ ,# 5" 7 <5< <1
4! !5 5 / 5 5 # 5 *5 / ,# 5 O5 3! 5 /5 *! #! %5 ; 5 5 '5 3! , 5 O5 . C #D 5 45 5 & # ( ! ( (!,! ! !# !, # # ($(# 5" 7 5& &
4! !55 # 5 *5/ 55/ ,# 5O53! 5/5*! #! %5;5 5'53! , 5O5. C #D 545258 8 3! (* $* / " # 4
3 7 B$(I 8 5 ' 5>
4 5/'55B D ( # ( ( % !# # @" $ ($ 5!% 831-5>- >--
4 5/'5B$ 5&=5',5O=5B ,5=H5< 25B# ( ),
@& $ # ( ! !# ,
($ 5=# (" !% >52>-2 2>1 4 5 / ' 9#,#!5 5 << 5 / ( ! $ , $ # ( 6% , (# 5=# (+ *% 2<511>>
;# 5 '5 =# # 5 3 '5 B D 5 '5 5 8 H5 +,5 ;5 " # 5 85 5 8 ($ %5 +# ) # ! !% 8 3 -5 1>
) !5T5" 5O5+ D 5;5 D 5 5+, !5"5; 5 5< >5 (# ,
@ ! !# ## ,(( $ ( # 5=# (" * %>5> >> = ,5 '5 !,5 =5 5 9 ( ,
, E % # 5 =# (
-5>>
= 5 *5 5 = "5 3 # !5 5 ;(( 5 = 5 ;, 5 = &5 <<25 " 8 B$ 7 ' '/ % 5 8 / ->5
O % 5475<<5'# (,
,#5<<5)9"D + #D85B9252 2
O 5 ' B5 <5 % ! ! 9 ( *A2 7 ! ! ! " A2 ,A 5 ! / /
5I %(B
' , , =55/
# ( ! # 7$%" ,@" 5!% 8315>--
' D 5 #DD 5=5< 5*2A $2A !6% ! 5=# ( !'
* 5> >-
O ) $55<< 5&8( !O &2A5+2A5T$2A *2AT+722U1;7 T7-2U ;7 , % @
#%(!% ( 5!% 325
+,#%5 5 >5 ! ( ## ! , ,
5 ! / /
5 ; * ,5 O , 5 I" !545D#C 5'54 5/'55/( 7 8 / @ ! ,%+" 7 )) # # 5 *53! 5/5/! 5"55853! , 5O5/ ,# 5O5<58 $! (!,! ! !#
6# ($ # , 5=# (+ *% 525-<1>
# 5 *5 5 85 3! 5 O5 / ,# 5 O5 <5 8 $! # ( " , ($ !,! 57 *# 5 > >
8%575 ,554 #!5=*5" $ 5'5/#
#5'53
V5=*5B 55<<>5" 7 B$ $ 7 % # '# (8 / 5 !) *(7 B$ 7BW<>5H $#,5."
9 5 /# 8;5<><5 ! ,%4
))5 #>+TD@"
H ,5 *5 ;#C# 5 X5 '5 X5 <<<5 '# ( ,,, 9 # 5 =# (
' 5 -<
ScienceDirect Procedia Materials Science 10 (2015) 683 – 692
) *(+ ! , *+ -
!"#
!"#$$% &' & ()))*+ , - $ $
! ( $ (
( # * *"# ! # ! ! ,
$ ($ !#,! ( ! # *./
# ! # , !0# , ! #%( ! $! # 1* , # 12 , ! !
%($ !* *"# ($ (# $-1-234% -2134%5 % ! 6 # ! ! * *"# ($ ! , 6 #!! $# (# (($ $ % $ © 2015 The!"# ! #$ !$%& ' Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). # $ %( !) *(+ ! , *+ - Peer-review under responsibility of the International Conference on Nanomaterials and Technologies (CNT 2014) './
7 ($5* "# ,
5,, 5/( 5)#
58
$ !
7 ($$ , ! !,! % #! # 5! 9 # ) ( !( ( , ! % ( (# ( ! 7 ($ $, % , % ( % $ (( !% (( ,
($ 5 # $ $ 6 ( # : ;# / % $$ !( ( #( , ,
: # < 4! ! 5 ! ( , ( 6 , 5 # $% ! % % # # ' 7' = <<25 8% <<> " ! % # ! (
!
# ( # ( ($ ($ % %
?* , # ! @A< 22 - 2 2:( 6@A< 22 ->2<> 0
1 , - $ $
2211-8128 © 2015 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). Peer-review under responsibility of the International Conference on Nanomaterials and Technologies (CNT 2014) doi:10.1016/j.mspro.2015.06.068
684
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
$ ( %5 % ! " 5#! ! ( % ($ ! ( # $ ! % ! %( $ ($ ! ((( #! 45 " 5 % :4! ! 5 = <<25 # <5 B$ < 4 # ($ !#! % ! ! (" ($ : # < ($ $ , ( # !#,! % %!,! 7# # %!,! ($ ! ! ( ($ 5!! $%(( (# % % # , ! ,! #C# D ; + ( , !12 ) ! ! * "# , # ! ! ,
$
% ($ $ !( ,( $# ! (* "# ,
*"# ,
! 6 ! ((%(,% (( !! ,
6 !
B# !5 * ,
! # ( ! !# !$ $ ! *7
,, 6 ( *2A *-A : * #! ( # ! ! ,
!* *"# !# %( ($ $ ) ! 5 ! # (* ($ ( % !#,! # (#
#$%(( D ( #%
! # ( !
! (* *"# , # ! ! ,
$ ($ !#,! ! ( *! . / *./ !0## ! # ,
, ! #%( ! $! ## 1* , # ! ! 9 # ( ! , ! (* *"# , ,
!#,! & 5 & &/E $ ! ,, (( ( * 5 ( ( # ! $! ( ($ # ! ( F % , ! #
! &8 #% ! $ ( , ($ ! $ ( ! ! (* ! # ! ! ,
$ ($ ! !,! %5, % ! ! ## % ( ,$! #6!$ , %! *"# ($ ! % ! , , % ! ! ## $! 5 #,, , %
&' (
(
! *./
# ! ! # , !0#! $# ( $ % ( ,,
$ ($ ( !
( ! # % , 7 !7 G* ! # , % 0# 9 #$# B 2, (# - ! #$ !D
( ! # % !#,! )8 % 87 -- * B7. 3 " -*5H * 5 I" ! # # %(G* %!# % ! !6% !%,$# 9 ! % ( ! % ! # % 6 ( ! ,
D, ! , 0## # , # $ ! ( (( " 5* "#((6 (-# B (* ( 5 # # $
, ! ( " * 2 1;7 ** 2 >;7 5 ! ( *"# 0# # ( " * 2 1;75 ** 2 >;7 "#* 2
! ( ## # % ! # , ( ! ! 8& : +,#% >5 ) ! < >5 $ ! ,8& # # #(8& ) 5 ! " ! (* , :" < 1 ! #$ ! D % ! # ,
D, ! ( $% !% 6 $% , ! # ( < >* B %5 ! #$! $ % ! ! ( !($ ( GJ! $ ( !( $ ( ! ! 5 # 5 ((
685
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
C# #! ! ! ! ! ! ( ! ! ( ! $ !( $ ! ! ! ( #$ ! # %: # < ! ( ! * *"# ($ ( $ $ /
@/ (( $ * / - *"# / ($
0
/ - /
(
1(.
7A7 *7A" 72
7A7 A*7A"#72A" 72
1
$ !
2
( ! (
& 3
!+
!6 # # # ! $! (*/ - *"#/ # ! ! ,
$ ($ $ : # <"$# , ! (($ # ( ! ( ! ( ! $% ! ,, ! $ ! ($ ! 1* , # # ! (( ( !($ ! $% %, !6 # ((( ! ,! # 0# 9H! , 5 ,! $ % GK ! ! ,! ,# ( !($ ! !- , ! ,5 # #6 ! 1* , # D ! ,% . # ! #
, ! % % # !(( #! 5 8 ! 12 ! ! ##
! 4%
4
! #( ! ,%( ( / - / !(( * "# 6 # , , & & ! ! ( ! ( $ ($ & , 8 &8 $ ($ E $ &8 D@ 3#D 3 @ "2 ( ! (8 ! $ #&/E % ((/ - / # ! ! ( B, , ! (* "# ! , , ( (( # ! ( ! ( (# $# K " 725 K 75 2 K *7 / - ($ ! ! , , ! / # K " 725 K 75 > K *75 K "#72 3 ! ! ($ # ,# # (# ( " ( # " L1 K " 72($( $ *)8 *4*8) # !6 ( ! % %
%% %%
*% *% )% )% "% "% % % % % % " ) * % " % " ) * % " & +,- . & +,- .
&/E ( (* *"# $($ (
B, ! ( ! ( ( $ ! ! ($ #
686
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
687
688
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
689
690
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
691
692
S. Ghosh et al. / Procedia Materials Science 10 (2015) 683 – 692
,
# !,! % ! #( (8 ! 8 ! !!,! %(* ($ -1-234% ! ! (*"# ($ -2134% ! % % ! # 12 " ! # ! ! ($ #! # $ ( ! ! ($
; < (
"# ! ! D ,/8/7 +/ !(( # ! # ! ! D(# ! O / ,# 5 / *)8 *4*8)(! ## # , 5,# # ! D
3
" 5O5+ D 5;5O# 5O ; 5 5< 15" ## ! !# ,(( !( # # # (%# ,
5=# (" !% <52-2 2-21
"$ , 5" 3 %535<>5& , 8 ( ) 576(5* 3 %53 5OH;5<25 , 58 ,!% 15 <
* 5*5 5 5 995B5 585* #5 5 # #5"5O 585 9955 ,!5"53 5 55 $ %( # # ! ,
($%$ ! !# 5=# (" *! % >5-1 -1<
B$ 5&=5!# 95*54,!5 &5< 5* (( ! (4 ($ ,# 5" 7 <5< <1
4! !5 5 / 5 5 # 5 *5 / ,# 5 O5 3! 5 /5 *! #! %5 ; 5 5 '5 3! , 5 O5 . C #D 5 45 5 & # ( ! ( (!,! ! !# !, # # ($(# 5" 7 5& &
4! !55 # 5 *5/ 55/ ,# 5O53! 5/5*! #! %5;5 5'53! , 5O5. C #D 545258 8 3! (* $* / " # 4
3 7 B$(I 8 5 ' 5>
4 5/'55B D ( # ( ( % !# # @" $ ($ 5!% 831-5>- >--
4 5/'5B$ 5&=5',5O=5B ,5=H5< 25B# ( ),
@& $ # ( ! !# ,
($ 5=# (" !% >52>-2 2>1 4 5 / ' 9#,#!5 5 << 5 / ( ! $ , $ # ( 6% , (# 5=# (+ *% 2<511>>
;# 5 '5 =# # 5 3 '5 B D 5 '5 5 8 H5 +,5 ;5 " # 5 85 5 8 ($ %5 +# ) # ! !% 8 3 -5 1>
) !5T5" 5O5+ D 5;5 D 5 5+, !5"5; 5 5< >5 (# ,
@ ! !# ## ,(( $ ( # 5=# (" * %>5> >> = ,5 '5 !,5 =5 5 9 ( ,
, E % # 5 =# (
-5>>
= 5 *5 5 = "5 3 # !5 5 ;(( 5 = 5 ;, 5 = &5 <<25 " 8 B$ 7 ' '/ % 5 8 / ->5
O % 5475<<5'# (,
,#5<<5)9"D + #D85B9252 2
O 5 ' B5 <5 % ! ! 9 ( *A2 7 ! ! ! " A2 ,A 5 ! / /
5I %(B
' , , =55/
# ( ! # 7$%" ,@" 5!% 8315>--
' D 5 #DD 5=5< 5*2A $2A !6% ! 5=# ( !'
* 5> >-
O ) $55<< 5&8( !O &2A5+2A5T$2A *2AT+722U1;7 T7-2U ;7 , % @
#%(!% ( 5!% 325
+,#%5 5 >5 ! ( ## ! , ,
5 ! / /
5 ; * ,5 O , 5 I" !545D#C 5'54 5/'55/( 7 8 / @ ! ,%+" 7 )) # # 5 *53! 5/5/! 5"55853! , 5O5/ ,# 5O5<58 $! (!,! ! !#
6# ($ # , 5=# (+ *% 525-<1>
# 5 *5 5 85 3! 5 O5 / ,# 5 O5 <5 8 $! # ( " , ($ !,! 57 *# 5 > >
8%575 ,554 #!5=*5" $ 5'5/#
#5'53
V5=*5B 55<<>5" 7 B$ $ 7 % # '# (8 / 5 !) *(7 B$ 7BW<>5H $#,5."
9 5 /# 8;5<><5 ! ,%4
))5 #>+TD@"
H ,5 *5 ;#C# 5 X5 '5 X5 <<<5 '# ( ,,, 9 # 5 =# (
' 5 -<