341
Related articles published in Journal of Chromatography, Vols. 626-632 Volume 626 On-line coupled reversed-phase high-performance liquid chromatography-gas chromatography-mass spectrometry. A powerful tool for the identification of unknown impurities in pharmaceutical products by J. Ogorka, G. Schwinger and G. Bruat (Basle, Switzerland) and V. Seidel (Grax, Austria) . . . . . . . . . . . Pharmaceutical applications of high-performance liquid chromatography ~~J.E.DiNunxio(BufFalo,NY,USA)
87
interfaced with Fourier transform infrared spectrosco-
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
97
Experimental design in the development and characterization of a high-performance liquid chromatographic method for amino acids by H. A. Hansen and C. Emborg (Lyngby, Denmark) . . . . . . . . . . , . . . . . . . . . . . . . . . . . 171 Investigation of the effect of acylation on the enantiomeric separation of amino acid isopropyl esters by gas chromatography by X. Lou, X. Liu, D. Zhu, Q. Wang and L. Zhou (Dahan, China) . . . . . . . . . . . . . . . . . . . . . . 231 Selective determination of secondary amino acids as their N-dimethylthiophosphoryl methyl ester derivatives by gas chromatography with tlame photometric detection by H. Kataoka, K. Nagao, N. Nabeshima, M. Kiyama and M. Makita (Okayama, Japan) . . . , . . . . . . . . 239 Application of capillary electrophoresis to pharmaceutical analysis. Determination of alendronate in dosage forms by E. W. Tsai, M. M. Singh, H. H. Lu, D. P. Ip and M. A. Brooks (West Point, PA, USA) . . . . . . . . . . . . 245 Determination and rotamer separation of enalapril maleate by capillary electrophoresis by X.-Z. Qin, D. P. Ip and E. W. Tsai (West Point, PA, USA) . . . . . . . . . . . . . . . . . . . . . . . . 251 Development of an assay for penicillin G in chinook salmon muscle tissue by R. G. Aoyama, D. D. Kitts, H. M. Burt and K. M. McErlane (Vancouver, Canada)
. . . . . . . . . . . . . 271
Volume 627 Use of chiral monohalo-s-triazine reagents for the liquid chromatographic resolution of DL-amino acids by H. Brtlcker and B. Strecker (Stuttgart, Germany) . . . . . . . . . . . . . . . . . . . . . . . . . . . ,
97
Immobilized metal ion aflinity chromatography of synthetic peptides. Binding via the a-amino group by P. Hansen, G. Lindeberg and L. Andersson (Uppsala, Sweden) . . . . . . . . . . . . , . . . . . . . . . 125 Use of monobromobimane to resolve recombinant proteins by reversed-phase high-performance liquid chromatography baaed on their cysteine content by D. 0. O’Keefe (Rahway, NJ, USA) and A. L. Lee and S. Yamaxaki (West Point, PA, USA) . . . . . . . . . . 137 Heterogeneous binding of aldolase to phosphocellulose. Interpretation in terms of a “concerted cluster” model of multivalent a&my by V. Dowd and R. J. Yon (London, UK) . . . . . . . . . . . . . . . . . . . . . . . . . . . . , . . . . 145 Purification, subunit structure and inhibitor profile of cathepsin A by J. J. Miller, D. G. Changaris and R. S. Levy (Louisville, KY, USA)
. . . . . . . . . . . . . . . . . . . . 153
Purification and determination of the binding site of lactate dehydrogenase from chicken breast muscle on immobilimd ferric ions by G. Chaga, L. Andersson and J. Porath (Uppsala, Sweden) . . . . . . . . . . . . . . . . . . . . . . . . 163 Separation of tetracycline and its degradation products by capillary zone electrophoresis by C.-X. Zhang, Z.-P. Sun, D.-K. Ling and Y.-J. Zhang (Beijing, China) . . . . . . . . . . . . . . . , . . . . 281 Determination of oxytetracycline in marine shellfish (Crassostrea gigas. Ruditapex phil~pinarum and Scrobicuiaria plana) by high-performance liquid chromatography using solid-phase extraction by H. Pouliquen, D. Keita and L. Pinault (Names, France) . . . . . . . . . . . . . . . . . . . . . _ . , . 287 Volume 628 Column liquid chromatography of cefadroxil on poly(styren~vinylbenzene) by C. Hendrix, C. Wijsen, L. M. Yun, E. Roets and J. Hoogmartens (Leuven, Belgium)
. . . . . . . . . . . . .
49
Relaied articles
342
Structural c&a+rimtion of polypept@ and proteins by combination of capillary electrophoresis and zssCfplasma deso@on ~~gpectt;dmetr by W. Weimnann, K. Baumeister, I. Kaufmann and M. Prxybylski (Konstanz, Germany) . . . . . . . . . . . . . 111 Packed-column supercritical fluid chromatography of omepraxole and related compounds. Selection of column support with triethylamine- and methanol-modifled carbon dioxide as the mobile phase by 0. Gyllenhaal and J. Vessman (Mdlndal, Sweden) . . . . . . . . . . . . . . . . . . . . . . . . . . . 275 Separation of polymyxins by mice&r electrokinetic capillary chromatography by H. K. Kristensen and S. H. Hansen (Copenhagen, Denmark) . . . . . . . . . . .
. . .
. . . . . . . 309
High-performance liquid chromatographlc determination of urinary 2,5-hexanedione by A. Sturaro, G. Parvoli and L. Doretti (Padova, Italy) . . , . . . . . . . . . . . . . . . . . . . . . . . . 316 v01u??te429 Disruption and fractionation of biological materials by matrix solid-phase dispersion by S. A. Barker, A. R. Long and M. E. Hines II (Baton Rouge, LA, USA) . . . . . . . . . . . . . . . . . . ,
23
High-performance liquid chromatography versus solid-phase extraction for post-derivatixation cleanup prior to gas chromatography-electron-capture negative-ion mass spectrometry of N1,N3-bis-(pentatluorobenxyl)-N7-(2-[pentaethyl)xanthine, a product derived from an ethylene oxide DNA adduct byM.SahaandR.W.Giese(Boston,MA,USA) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
35
Application of solid-phase extraction in the determination of U-82217 in rat serum, urine and brain byW.Z.Zhong(Kalamazoo,MI,USA) . . . . . . . . . . . . . . . . . . . . . . . , . . . . . . . .
83
High-performance liquid chromatographic method for the determination of dimethindene in urine by D. Chollet, P. Kilnstner and M. Wermeille (Nyon, Switzerland) . . . . . . . . . . . . . . . . . . . . . .
89
Reversed-phase high-performance liquid chromatography for evaluating the lipophilicity of pharmaceutical substances with ionization up to log PFpp = 8 by K. Belsner, M. Pfetfer and B. Willfert (Neuss, Germany) . . . . . . . . . . . . . . . . . . . . . . . . 123 Chemometrics in bioanalytical sample preparation. A fractionated combined mixture and factorial design for the modelling of the recovery of five tricyclic amines from plasma after liquid-liquid extraction prior to high-performance liquid chromatography by J. Wieling (Zuidlaren and Groningen, Netherlands), H. Dijkstra, C. K. Mensink and J. H. G. Jo&man (Zuidlaren, Netherlands) and P. M. J. Coenegracht, C. A. A. Duineveld and D. A. Doombos (Groningen, Netherlands) . . . . 181 Novel affinity separations based on perfluorocarbon emulsions. Development of a perfluorocarbon emulsion reactor for continuous alhnity separations and its application in the purification of human serum albumin from blood plasma by G. E. McCreath, H. A. Chase, D. R. Purvis and C. R. Lowe (Cambridge, UK) . . . . . . . . . . . . . . . . 201 Enantiospecific drug analysis via the orrho-phthalaldehyde/homochiral thiol derivatixation method byD.M.DesaiandJ.Gal(Denver,CO,USA) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 215 Liquid chromatographic determination of amoxicillin preparations. Interlaboratory validation by H.-C. Chung and M.-C. Hsu (Taipei, Taiwan) . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . 277
vohle 630 Determination of hyaluronic acid by high-performance liquid chromatography of the oligosaccharides derived therefrom as I-(4methoxy)phenyl-3-methyl-5-pyraxolone derivatives byK.Kakehi,M.Ueda,S.SuxukiandS.Honda(Osaka,Japan) . . . . . . . . . . . . . . . . . . . . . . 141 Separation and isolation of trace impurities in L-tryptophan by high-performance liquid chromatography byM.W.Trucksess(Washington,DC,USA) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 147 Quantitative analysis of tylosin by column liquid chromatography by E. Roets, P. Beirinckx, I. Quintens and J. Hoogma&ns
(Leuven, Belgium)
. . . . . . . . . . . . . . . . . 159
Determination of the number and relative molecular mass of subunits in an oligomeric protein by twodimemional electrophoresis. Application to the subunit structure analysis of rat liver amidophosphoribosyhransferase by T. Yamaoka and K. Yamashita (Ibaraki, Japan) and M. Itakura ~okushima City, Japan) . . . . . . . . . . . 345 Separation of drug stereoisomers by capillary electrophoresis with cyclodextrins byT.E.Peterson(FortWorth,TK,USA) , . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 353
343
Related articles
Separation and simultaneous determination of the active ingredients in theophylline tablets by micellar electrokinetic capillary chromatography by Q.-x. Dang and L.-x. Yan (Xian, China) and Z.-p. Sun and D.-k. Ling (Beijing, China) . . . . . . . . . . . . 363 Determination of acidic saponins in crude drugs by high-performance liquid chromatography on octadecylsilyl porous glass by H. Kanazawa, Y. Nagata, Y. Matsushima, M. Tomoda and N. Takai (Tokyo, Japan) . . . . . . . . . . . . . 408 Capillary electrophoretic separation of recombinant granulocyte-colony-stimulating factor glycoforms by E. Watson and F. Yao (Thousand Oaks, CA, USA) . . . . . . . . . . . . . . . . . . . . . . . . . . . 442 v01unle 631 Analytical and preparative high-performance liquid chromatographic separation of thienopyran enantiomers by C. J. Shaw, P. J. Santilippo, J. J. McNally, S. A. Park and J. B. Press (Raritan, NJ, USA) . . . . . . . . . . . 173 Direct chit-al separation of almokalant on Chiralcel OD and Chiralpak AD for liquid chromatographic assay of biological samples by K. Balm&r, P.-O. Lagerstrom, S. Larsson and B.-A. Persson (Miilndal, Sweden) . . . . . . . . . . . . . 191 Determination of ephedrines in urine by high-performance liquid chromatography by C. Imaz, D. Carreras, R. Navajas, C. Rodriguez, A. F. Rodriguez, J. Maynar and R. Cortes (Madrid, Spain) .
. 201
Porous graphitized carbon and octadecylsilica columns in the separation of some monoamine oxidase inhibitory drugs by E. Forg&cs, K. Valko, T. Cserhati and K. Magyar (Budapest, Hungary) . . . . . . . . . . . . . . . . . . . 207 Liquid chromatography-mass spectrometry for the determination of medetomidine and other anaesthetics in plasma by H. Kanazawa, Y. Nagata, Y. Matsushima, N. Takai, H. Uchiyama, R. Nishimura and A. Takeuchi (Tokyo, Japan)
215
Reversed-phase high-performance liquid chromatography of the cardiac glycoside LNF-209 with refractive index detection by P. H. Zoutendam, D. L. Berry and D. W. Carkti (Norwich, NY, USA) . . . . . . . . . . . . . . . . 221 Determination of oxiracetam in human plasma by reversed-phase high-performance liquid chromatography detection by R. C. Simpson, V. K. Boppana, B. Y.-H. Hwang and G. R. Rhodes (King of Prussia, PA, USA)
with fluorimetric
. . . . . . . . 227
Column-switching high-performance liquid chromatographic method for the determination of SK&F 106203 in human plasma after fluorescence derivatization with 9-anthryldiazomethane by C. Miller-Stein, B. Y.-H. Kwang, G. R. Rhodes and V. K. Boppana (King of Prussia, PA, USA) . . . . . . . 233 Determination of baicalin and puerarin in traditional Chinese medicinal preparations by high-performance liquid chromatography by K.-C. Wen, C.-Y. Huang and F.-L. Lu (Taipei, Taiwan) . . . . . . . . . . . . . . . . . . . . . . . . 241 Normal-phase high-performance liquid chromatographic determination of epristeride, a prostatic steroid Sa-reductase enzyme inhibitor, in human plasma by V. K. Boppana, C. Miller-Stein and G. R. Rhodes (King of Prussia, PA, USA) . . . . . . . . . . . . . . . . 251 Rapid, sensitive high-performance liquid chromatographic method for the quantification of promethazine in human serum with electrochemical detection by A. R. Fox and D. A. McLaughlin (Baltimore, MD, USA) . . . . . . . . . . . . . . . . . . . . . . . 255 High-performance liquid chromatography of human glycoprotein hormones by M. A. Chlenov, E. I. Kandyba, L. V. Nagornaya, I. L. Orlova and Y. V. Volgin (Moscow, Russian Federation) Separation of interleukins by a preparative chromatofocusing-like method by S. P. Monkarsh, E. A. Russoman and S. K. Roy (Nutley, NJ, USA)
. 261
. . . . . . . . . . . . . . . . . . . . 277
Volume 632 Isolation of plasma proteins from the clotting cascade by heparin afllnity chromatography byD. JosiC,F.BalandH.Schwinn(Vienna,Austria) . . . . . . , . . . . . . . .
. . . ,
. . . . . . .
Conformational changes of brain-derived neurotrophic factor during reversed-phase high-performance liquid chromatography by R. Rosenfeld and K. Benedek (Thousand Oaks, CA, USA) . . . . . . . . . . . . . . . . . . . . . .
29
Estimation of the extent of lipid peroxidation in the ischemic and reperfused heart by monitoring lipid metabolic products with the aid of high-performance liquid chromatography by G. A. Cordis and N. Maulik (Farmington, CT, USA), D. Bag&i (Omaha, NE, USA) and R. M. Engelman and D. K. Das (Farmington, CT, USA) . . . . . . . . . . . . . . . . . _ . . . . . . . . . . . . . . . . . , . . .
97
344 Separation of metallothionein isoforms by capillary zone electrophoresis by J. H. Beattie (Aberdeen, UK), M. P. Richards (Reltsville, MD, USA) and R. Self (Aberdeen, UK)
Related articles
. . . . . . . 127
Determination of ten B-blockers in urine by mice&u electrokinetic capillary chromatography by P. Lukkari, H. Siren, M. Pantsar and M.-L. Riekkola (Helsinki, Finland) . . . . . . . . . . . . . . . . . . 143 Determination of sulphonamides in pharmaceuticals by capillary electrophoresis by C. L. Ng, H. K. Lee and S. F. Y. Li (Singapore, Singapore) . . . . . . . . . . . . . . . . . . . . . . . . 165 On-line sample preconcentration on a packed-inlet capillary for improving the sensitivity of capillary electrophoretic analysis of pharmaceuticals byM.E.SwartzandM.Merion(Milford,MA,USA) . . . . . . . . . . . . . . . . . . . . . . . . . . . , 209 Screening of B-blockers in human serum by ion-pair chromatography and their identification as methyl or acetyl derivatives by gas chromatography-mass spectrometry by H. Siren, M. Saarinen, S. Hainari, P. Lukkari and M.-L. Riekkola (Helsinki, Finland) . . . . . . . . . . . . 215